Optimized Route for the Synthesis of Derivative of Phenylalanine-azobenzene
Jie Chen, Gao He, Liangchun Li
International Research Journal of Pure and Applied Chemistry · pp. 1–5 · Published 22 Apr 2019
10.9734/irjpac/2019/v18i430095Abstract
In this paper, the derivative of phenylalanine-azobenzene was synthesized from p-nitrobenzoic acid and L-ethyl benzoate by condensation, ferric acid reduction and aromatic amine oxidation, and the key compounds were characterized by 1H-NMR and MS. At the same time, we optimized the synthetic route. And the optimized route increased the total yield of target molecule by 10.28%.
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