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All published articles 998

New Heat-Proof Methylphenylsiloxane Resins and High Temperature Resisting Enamels on Their Basis

O. G. Ryzhova, A. M. Kontorov, A. N. Polivanov, R. S. Mirgazitova & A. I. Katanaev · International Research Journal of Pure and Applied Chemistry · 2014

New heat resistant methylphenylsiloxane resins produced by methyltriethoxysilane and oligophenylsilsesquioxane acidolysis were investigated. The synthesized resins are characterized by narrow molecular-mass distribution, higher thermal and thermal oxidative stability, reduced gel...

Open access Research Article 10.9734/IRJPAC/2014/7257

Separation of Palmitic and Palmitoleic Acid and their FAMEs using Transition Metal Salts

Sayali Kulkarni & Sandun Fernando · International Research Journal of Pure and Applied Chemistry · 2014

Fatty acids (FAs) play an important role in physiological functions. Hence, separation and isolation of FAs is of great industrial importance. With the intension of finding out effective means of separating different forms of lipid constituents, two studies were carried out. In t...

Open access Research Article 10.9734/IRJPAC/2014/9869

RP-HPLC Determination of Benzoic Acid in Samples of Children Food Distributed in Aden-Yemen

A. M. Saeedan, S. Kh. Bamoteref & M. A. Algahri · International Research Journal of Pure and Applied Chemistry · 2014

Reverse phase high-performance liquid chromatographic method that allows the determination of the preservative benzoic acid is described. Separations were affected by using an initial mobile phase of methanol–acetate buffer (pH 4.4), (35:65). Separation of benzoic acid is achieve...

Open access Research Article 10.9734/IRJPAC/2014/8720

Synthesis of NiO Nanoparticles by Water-in-oil Microemulsion Technique

Prakash Palanisamy & Ashok M. Raichur · International Research Journal of Pure and Applied Chemistry · 2014

NiO nanoparticles were synthesized by water-in-oil microemulsion technique using Aerosol-OT as a surfactant. The study aims to understand the nanoparticle size and distribution synthesized with the surfactant and co-precipitated without surfactant. Nanoparticles were synthesized...

Open access Research Article 10.9734/IRJPAC/2014/8538

Distribution Pattern of the Heavy Metals: Pb, Zn, Cd and Cu in Roadside Soils of Maiduguri Metropolis, Borno State Nigeria

S. T. Garba, I. Ahmed, J. C. Akan & B. A. Dauda · International Research Journal of Pure and Applied Chemistry · 2014

In this research work the level of the metals: Pb, Cd, Zn, and Cu were determined in soil samples collected within Maiduguri Metropolis. Samples were collected from places of high anthropogenic activity such as automobile maintenance workshop (AMW), Car park or Bus stops (CP), an...

Open access Research Article 10.9734/IRJPAC/2014/9924

A Rapid Spectrophotometric Method for the Determination of Trace Level Silver Using 1, 5-diphenylthiocarbazone in Aqueous Micellar Solutions

M. Jamaluddin Ahmed & Syeda Rahimon Naher · International Research Journal of Pure and Applied Chemistry · 2014

The very sensitive, fairly selective direct spectrophotometric method is presented for the rapid determination of silver at ultra-trace level using1, 5-diphenylthiocarbazone (dithizone) as a new micellar spectrophotometric reagent ( max= 495 nm) in a slightly acidic (0.1-1.0 M H2...

Open access Research Article 10.9734/IRJPAC/2014/8157

Isolation, Structural Elucidation and Anti-Lipid Peroxidation Activity of 3-(5-Hydroxy-2-(4-Hydroxyphenyl)-4-Methyl-Chromen-3-Yl) Propanoic Acid from the Stem Bark of Brachystegia eurycoma Harms

O. U. Igwe & J. O. Echeme · International Research Journal of Pure and Applied Chemistry · 2014

Aim: To isolate, characterize and ascertain the anti-lipid peroxidation activity of a chromene propanoic acid from the stem bark of Brachystegia eurycoma Harms. Study Design: The study was designed to search, isolate and elucidate the structure of a novel compound and then test i...

Open access Research Article 10.9734/IRJPAC/2014/8594

Characterization of Bioactive Sesquiterpenes, Organic Acids and Their Derivatives from the Leaves of Psidium guajava Linn

Okenwa U. Igwe & T. Abii · International Research Journal of Pure and Applied Chemistry · 2014

The isopropanolic extract of the leaves of Psidium guajava Linn was analyzed by Gas chromatography-mass spectrometry (GC-MS). Fourteen different phytochemical compounds have been characterized, including 1, 3, 3-trimethyl-2-oxabicyclo [2.2.2] octane, (2.06%), 4, 11, 11-trimethyl-...

Open access Research Article 10.9734/IRJPAC/2014/8592

Physico-chemical Quality of Drinking Water in New Bussa, Niger State, Nigeria

J. C. Nnaji & S. Omotugba · International Research Journal of Pure and Applied Chemistry · 2014

The study assesses the physico-chemical parameters and metal concentrations in drinking water from different sources in New Bussa, Niger State, North Central Nigeria. Triplicate Water samples were collected from 12 sampling points located all over the town including a well, boreh...

Open access Research Article 10.9734/IRJPAC/2014/7289

The Electrical Breakdown Characteristics of the Water Vapor in Micrometer Gap Sizes

Branislav Radjenović, Marija Radmilović-Radjenović, Š. Matejčik, M. Klas & P. Beličev · International Research Journal of Pure and Applied Chemistry · 2014

The liquid water-metal interface and the liquid water-gas interface, both play an important role in the initiation and the development of the electrical discharge in the gas bubbles. Evidence from the environmental application studies supports the strong dependence of the dischar...

Open access Research Article 10.9734/IRJPAC/2014/8550

Comparative Studies of Heavy Metals in Mine Water by Square Wave Stripping Voltammetry and Atomic Spectroscopy

S. Uba, B. R. Horrocks, A. Uzairu, M. S. Sallau & H. Abba · International Research Journal of Pure and Applied Chemistry · 2014

Inductively coupled plasma- optical emission spectroscopy (ICP-OES) and square wave voltammetry (SWV) were used to analyse and compare the concentrations of Cu, Cd, Hg, Pb and Zn in polluted mine water samples from Shilbottle in North Eastern England, United Kingdom. The results...

Open access Research Article 10.9734/IRJPAC/2014/8283

Electrochemical Decolorization of Maxilon Red GRL Textile Dye

Gamal O. El-Sayed, Mohamed S. Awad & Zahraa A. Ayad · International Research Journal of Pure and Applied Chemistry · 2014

Aims: The aim of this research paper is to examine the efficiency of electrooxidation and electrocoagulation techniques to remove the textile dye Maxilon Red GRL from polluted water. Study Design: The study was performed by using two graphite electrodes as anode and cathode for e...

Open access Research Article 10.9734/IRJPAC/2014/7819

Synthesis and Structure-property Relations in Ce4-xCa1+xFe5-xZnxO14+δ (0≤x≤0.45) (T1-T4: x=0, 0.15, 0.30 and 0.45) Oxide Systems

B. B. Das, Thangaraj . & Deepa . · International Research Journal of Pure and Applied Chemistry · 2014

Synthesis of the composition Ce4-xCa1+xFe5-xZnx O14+δ (0≤ x ≤0.45) (T1-T4: x=0, 0.15, 0.30 and 0.45) were done via nitrate-citrate gel route. The wavelength of X-rays is on the atomic scale, so X-ray diffraction (XRD) is a primary tool for probing structure of nano-materials. Cry...

Open access Research Article 10.9734/IRJPAC/2014/7586

Chemical Constituents of the Leaf, Stem, Root and Seed Essential Oils of Aframomum melegueta (K. Schum) from South West Nigeria

I. A. Owokotomo, O. Ekundayo & B. J. Oguntuase · International Research Journal of Pure and Applied Chemistry · 2014

Aframomum melegueta leaf, stem, root and seed essential oils were obtained by hydro-distillation and were analyzed by means of gas chromatography/mass spectrometry (GC/MS). Twenty components were identified in the leaf essential oil. The major components were mrytenyl acetate (29...

Open access Research Article 10.9734/IRJPAC/2014/7397