Controlled Catalytic Reduction in Synthesising Pure Tetrahydrocurcumin
Chandra Sekhara Rao Nethinti, Dhanraj T. S. S. Sundaram, Sarvesh Kumar, Sreenivasulu Boju, Raghu Babu Korupolu, Annapurna Nowduri, Uttam Kumar Ray
Asian Journal of Chemical Sciences · pp. 46–53 · Published 25 Mar 2022
10.9734/ajocs/2022/v11i219120Abstract
Pd-Catalyzed hydrogenation process has been developed to synthesize tetrahydrocurcumin from synthetic curcumin. Use of diphenyl sulphide as catalyst poison is crucial for lowering the activity of the catalyst and thus reduces impurity formation. The process avoids column chromatography to achieve good quality tetrahydrocurcumin in cost effective manner. All the prepared compounds are characterized by FT-IR, 1H NMR, mass and HPLC techniques.
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